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This chapter starts with a brief background required to set the stage for the design and engineering of 2D heterostructures for photovoltaic applications. It presents an overview of the 2D materials used in solar cells, their heterostructures, and their fundamental optical and. The strategies of heteroatomic substitution and configuration modulation in self-assembled materials (SAMs) are promising to advance perovskite solar cells (PSCs). Herein, we developed a novel β-position thiophene-substituted SAM (β-Th-2PACz) as a hole-selective layer (HSL) for inverted PSCs. NASA researchers have developed a novel process for assembling thin-film solar cells into larger solar arrays.
